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Extra resources for Asymmetric Synthesis II: More Methods and Applications
Osselton, E. M. , Krijnen, E. S. , Lodder, G. , and Cornelisse, J. (1988) Recl. Trav. Chim. Pays-Bas. , 107, 407–411; (b) Srinivasan, R. , Merritt, V. Y. , and Subrahmanyam, G. (1974) Tetrahedron Lett. , 32, 2715–2718; (c) Srinivasan, R. and Ors, J. A. (1976) Chem. Phys. Lett. , forty two, 506–508; (d) Ors, J. A. and Srinivasan, R. (1977) J. Org. Chem. , forty two, 1321–1327; (e) Jans, A. W. H. , Van Dijk-Knepper, J. J. , and Cornelisse, J. (1982) Recl. Trav. Chim. Pays-Bas. , a hundred and one, 275–276. sixteen. reports: (a) Corey, E. J. and Guzman-Perez, A. (1998) Angew. Chem. Int. Ed. , 37, 388–401; (b) Christoffers, J. and Barto, A. (2005) Quaternary Stereocenters, Wiley-VCH Verlag GmbH, Weinheim; For a few contemporary syntheses of chiral quaternary facilities, see: (c) Adhikari, S. , Caille, S. , Hanbauer, M. , Ngo, V. X. , and Overman, L. E. (2005) Org. Lett. , 7, 2795–2797; (d) Sklute, G. and Marek, I. (2006) J. Am. Chem. Soc. , 128, 4642–4649; (e) Sibi, M. P. and He, L. (2006) Synlett, 689–692; (f) Lee, ok. S. , Brown, M. ok. , Hird, A. W. , and Hoveyda, A. H. (2006) J. Am. Chem. Soc. , 128, 7182–7184; (g) Martin, D. , Kehrli, S. d'Augustin, M. , Clavier, H. , Mauduit, M. , Alexakis, A. (2006) J. Am. Chem. Soc. , 128, 8416–8417; (h) Soorukram, D. and Knochel, P. (2007) Org. Lett. , nine, 1021–1023, and references mentioned therein; (i) Nibbs, A. E. , Baize, A. L. , Herter, R. M. , and Scheidt, ok. A. (2009) Org. Lett. , eleven, 4010–4013. 17. basic experiences: (a) Wittig-type olefination: Kelly, S. E. (1991) in finished natural Synthesis (eds B. M. Trost and that i. Fleming), Vol. 1 (ed. S. L. Schreiber), Pergamon, Oxford, p. 729; (b) sp2-sp3-coupling: Tamao, ok. (1991) accomplished natural Synthesis (eds B. M. Trost and that i. Fleming), Vol. three (ed. G. Pattenden), Pergamon, Oxford, p. 435; (c) Claisen rearrangement: Ziegler, F. E. (1988) Chem. Rev. , 88, 1423–1452; (d) Hiersemann, M. and Nubbemeyer U. (eds) (2007) The Claisen Rearrangement, Wiley-VCH Verlag GmbH, Weinheim, p. 571; (e) For a up to date review of obtainable technique: Prantz, okay. and Mulzer, J. (2009) Angew. Chem. Int. Ed. , forty eight, 5030–5033. bankruptcy 23 Catalyst-Controlled 1,3-Polyol Syntheses Tobias Harschneck and Stefan F. Kirsch Polyketidetype traditional items are a category of molecules that provoke not just with their structural variety but additionally with a tremendous diversity of organic actions together with cytostatic, antibiotic, antifungal, and immunosuppressive homes . one of many key structural parts of those usual items are 1,3-polyol devices. within the biosynthesis of polyketides, an iterative C2-elongation of acetyl or propionyl starter devices by means of decarboxylative condensation with malonyl-CoA extender devices happens. Stereoselective relief of the carbonyl offers each attainable diastereoisomer . Taking this effective technique as a task version, various artificial methodologies towards 1,3-polyols  that mimic the iterative technique of nature were constructed up to now a long time. between those, some of the most often used equipment for the synthesis of 1,3-polyol arrays is the stereoselective allylation of aldehydes with boron allyl reagents built via Brown and Jadhav .